简介：Duetotheirsize-dependentpropertiesandflexibleprocessingchemistry(Alivisatos,1996),monodispersednanocrystalshaveattractedconsiderableattentionfortheirdistinguishedroleinfundamentalstudiesandtechnicalapplications.AlthoughmuchhasbeenreportedonfabricationofmonodispersedinorganicnanocrystalssuchasFe2O3,CdSe,PbSeandZrO2(Peng&Peng,2002;Zhuetal.,2002;Niederbergeretal.,2002;Pangetal.,2001),littlepublishedonthepreparationofBaSO4nanocrystalsandtheircrystalsizeandmorphologywhichaffecttheirperformanceinapplication.PolymeradditiveswithcomplexfunctionshavebeenusedastemplatestodirectorientednucleationandgrowthofBaSO4(Xiaoetal.,2001;Yuetal.,2002;Summersetal.,2002),asanewclassoffunctionalpolymers,theso-calleddouble-hydrophilicblockcopolymers,designedtocontrolthemorphologyofBaSO4(Colfenetal.,2002),includingtheirnanofiberssynthesizedinAOTmicroemulsion(Li&Mann,2000).ThoughsomuchresearchhasbeendevotedtocontrollingtheBaSO4morphologies,thepresentnotewillreportonthesynthesisofBaSO4nanocrystalswithsizecontrolling.

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简介：Well-dispersedBaSO4nanoparticlesweresynthesizedinthepresenceofsodiumpolyacrylate（PAAS）byasimpleprecipitationmethod,withBaCl2and（NH4）2SO4asreactants.ThedifferentrolesperformedbyPAASinthesynthesisofBaSO4nanoparticleswereinvestigatedusingX-raydiffractometry,Fouriertransforminfraredspectroscopy,andtransmissionelectronmicroscopy.TheresultsindicatethattheassynthesizedBaSO4nanoparticlesweresphereswithanaveragediameterof30nmandthattheirsurfaceswereaffectedbythePAAS.Underatypicalprocedureemployed,PAASreactedwithBaCl2toyieldanintermediate,servingasacontrolreleasingagentandseparatingthenucleationandcrystalgrowthprocessesoftheBaSO4nuclei.DuringformationoftheBaSO4nanospheres,theintermediateslowlydissolvedandreleasedbariumandpolyacrylateions,inhibitingthegrowthandaggregationofnewlyformedBaSO4seedsandresultinginparticlesofnarrowdiameterdistributionandimproveddispersibility.Moreover,thesepolyacrylateionsfurthermodifiedthesurfacesoftheBaSO4nanoparticles.

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简介：Fatiguepropertiesofage-hardenedAlalloy2017-T4underultrasonicloadingfrequency(20kHz)wereinvestigatedandcomparedwiththeresultsunderconventionalloadingofrotatingbending(50Hz).Thegrowthofacrackretardedatabout500μminsurfacelengthunderultrasonicloading,whileatabout20μmunderrotatingbending.Althoughstriationsbeingatypicalfracturemechanismwereobservedunderconventionalloading,mostoffracturesurfacewascoveredwithmanyfacetsunderultrasonicloading.Thesefacetswerealsoobservedunderrotatingbendinginnitrogengas.Thedifferenceingrowthmechanismdependingontheloadingfrequencyandtheretardationofacrackgrowthunderultrasonicloadingmaybecausedbytheenvironmentatthecracktipduetohighcrackgrowthrateunderultrasonicloading.

简介：TheinfluenceofNa2SO4ontheformationofZnOwhiskerswasinvestigatedinthispaper.ZnOwhiskerswithaspectratiosofupto50weresynthesizedbydissolvingε-Zn（OH）2precursorinNaOH/Na2SO4solutionatroomtemperature,followedbyagingoftheresultingsolutionat140℃for6h.Fouriertransforminfraredspectroscopy,Ramanspectroscopy,andX-rayphotoelectronspectroscopyanalysesrevealedthatSO42-ionswereprimarilyadsorbedonthe（100）planeoftheZnOwhiskersviaanouter-spherecomplexconfiguration（O-H…O）,therebypromotingtheone-dimensionalgrowthofZnOwhiskersalongthec-axis.

简介：有从30～80nm的尺寸的Fe3O4nanoparticles被湿milling铁粉末在一家行星的球工厂综合。阶段作文和同样综合的产品的形态学被X光检查衍射(XRD)测量，扫描电子显微镜学(SEM)和传播电子显微镜学(TEM)。NanosizedFe3O4粒子被湿milling准备金属性的铁粉末(?200网孔，99%)在与不锈钢装备的一家行星的球工厂，使用的小瓶与50:1并且以300rpm的旋转速度的ball-to-powder团比率在提取的水下面熨球。在这个方法的铁球的使用在Fe3O4formation起了一个关键作用。现在的技术简单，这个过程是容易的执行。

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简介：Octahedron-likeBaMoO4microcrystalsweresynthesizedbytheco-precipitationmethodatroomtemperatureandprocessedinmicrowave-hydrothermalat413Kfordifferenttimes(from30minto5h).ThesemicrocrystalswereanalyzedbyX-raydiffraction(XRD),field-emissiongunscanningelectronmicroscopy(FEG-SEM)andtransmissionelectronmicroscopy(TEM).XRDpatternsshowedthatthismaterialpresentsatetragonalstructurewithoutthepresenceofdeleteriousphases.FEG-SEMandTEMmicrographsrevealedthattheBaMoO4microcrystalspresentanoctahedron-likemorphologywithagglomeratenatureandpoly-disperseparticlesizedistribution.Thesemicrographsalsoindicatedthatthemicrocrystalsgrowalongthe[001]direction.Theobservedcrystallographicplanesinthesestructuresweremodeledcomputationallyandacrystalgrowthmodelwasproposedinordertoexplainthemorphologicalchangesasafunctionofprocessingtime.

简介：TiO2nanoparticlesweresynthesizedbyahomogeneouscontrolledprecipitationmethodusingindustrialtitaniumsulfate(Ti(SO4)2).TheobtainedpowderswerecharacterizedbyX-raydiffraction(XRD),transmissionelectronmicroscope(TEM),Fouriertransforminfraredspectroscopy(FTIR)andICPplasmaspectrometer.EDTAwasusedascomplexingagenttoimprovethepurityandtheformationofTiO2nanoparticles.Experimentalresultsindicatedthatthehigh-purityTiO2nanoparticleswere20nminmeansizeandnearlymonodispersed.

简介：Liquid-solid(L-S)masstransfercoefficients(Ks)werecharacterizedinagas-liquid-solid(G-L-S)three-phasecountercurrentmagneticallystabilizedbed(MSB)usingamorphousalloySRNA-4asthesolidphase.Effectsofsuperficialliquidvelocity,superficialgasvelocity,magneticfieldstrength,liquidviscosityandsurfacetensionwereinvestigated.ExperimentalresultsindicatedthattheexternalmagneticfieldincreasedKsinthree-phaseMSB,ascomparedtothoseinconventionalG-L-Sfluidizedbeds;thatKsincreasedwithmagneticfieldstrength,superficialgasandliquidvelocitiesanddecreasedwithliquidviscosityandsurfacetension;andthatKsshoweduniformaxialandradialdistributionsexceptforsmallincreasesclosetothewall.DimensionlesscorrelationswereestablishedtoestimateKsoftheG-L-ScountercurrentMSBusingSRNA-4catalyst,withanaverageerrorof3.6%.

简介：Thispaperestablishesanon-linearfiniteelementmodel(NFEM)ofL4-L5lumbarspinalsegmentwithaccuratethree-dimensionalsolidligamentsandintervertebraldisc.Forthepurpose,theintervertebraldiscandsurroundingligamentsaremodeledwithfour-nodalthree-dimensionaltetrahedralelementswithhyper-elasticmaterialproperties.Puremomentof10N·mwithoutpreloadisappliedtotheuppervertebralbodyundertheloadingconditionsoflateralbending,backwardextension,torsion,andforwardfle...

简介：提出了一种改进的圆锥优化算法,对传统圆锥优化算法的周期项进行了二次优化。首先,根据经典圆锥运动建立了二次优化的误差准则;其次,给出了推导二次优化补偿系数以及相应的残留误差的一般方法;最后,在不同的经典圆锥运动环境下对三例改进算法的姿态解算误差进行了仿真验证。结果表明,通过改进的四子样和五子样算法得到姿态解算精度与通过旋转矢量变化量的理想值得到的结果几乎完全一致。此外,由于比改进的五子样算法少一次叉乘和两次加法运算,而且仿真速度大约快14%,所以改进的四子样算法更值得推荐采用。

简介：在Mach数3.4的来流条件下,对二维后台阶流动精细结构开展了实验研究.实验分为后台阶上游无控制加粗糙带扰动及微涡流发生器（micro-vortexgenerator,MVG）扰动3种状态,采用基于纳米示踪的平面激光散射（nano-tracerbasedplanarlaserscattering,NPLS）方法获得了流向和展向切面内的高时空分辨率流动显示图像,并测量了模型表面静压分布.对大量NPLS图像取平均,研究了流场结构的时间平均规律,对比不同时刻的瞬态流场精细结构图像,发现不同状态下的湍流大尺度结构的特征时间.有粗糙带状态相对无粗糙带台阶下游回流区压力更低,而下游压力较高,台阶上游区别不大;受MVG控制后台阶下游附近区域压力突增;MVG对流动的控制改变能力较强,粗糙带能调整台阶上下游附近流动平稳过渡,流场壁面压力没有突变.

简介：介绍了光纤陀螺寻北的基本原理，分析了基座的倾斜误差对寻北精度的影响。基座平面绕垂直于陀螺轴的倾角将直接引起一个同样量级的方位角测量误差，从而在较大程度上影响寻北精度。基座平面绕陀螺轴的倾角对方位角测量的影响小，在一些寻北精度要求不高的场合，可以忽略该倾角的影响。最后介绍了光纤陀螺寻北仪的二位置寻北方案。二位置寻北方案利用光纤陀螺对相差180°的两个方向上的地球自转角速率水平分量的敏感，精确地解算出地理真北方向与陀螺轴向的夹角。系统简单，比较容易实现。

简介：针对CNS/INS组合导航系统中缩短初始对准时间的问题,设计了一种CNS/INS组合导航系统组合对准新方法。在CNS/INS姿态四元数组合算法的基础上,推导CNS/INS组合系统线性化状态方程,分析了INS和CNS姿态四元数差值构建量测方程。利用递推最小二乘原理实现了对该组合系统的信息融合,设计了基于该估计原理的组合导航系统初始对准方法,考虑到大气层内动基座条件下对于星敏感器造成的干扰因素增加了加权处理环节,最后通过仿真实验验证了递推加权最小二乘法在处理组合导航系统初始对准中的有效性。仿真结果表明在微晃基座条件下,与传统的滤波方法相比较该估计方法能够有效地缩短约25%的对准时间。

简介：《中国惯性技术学报》编辑委员会第二次工作会议于1993年5月27日～29日在天津召开,参加会议的有编委会主任委员陆元九,学会领导高寿祖,副秘书长魏兰.副主任委员汪顺亭、章燕申、孙肇荣以及编委和编辑部的成员共21人。会议由副主任委员汪顺亭主持,707所所长张宗洵、副所长熊正南、情报室主任戴惠霞到会表示祝贺,并对707所为《学报》编辑部和学术交流部工作的同志表示大力支持。陆元九主任

简介：可调谐二极管激光吸收光谱技术是一种非接触的光谱诊断技术,已经广泛应用于高温气动研究中.文章对吸收光谱的发展和应用于高温反应环境温度和组分浓度的测量进行了回顾.对不同的吸收测量策略以及相应的系统组成进行了详细介绍,最后介绍了应用吸收光谱技术研究超声速燃烧火星再入以及空间推进系统的详细结果.