简介:Lowtemperaturecompositechromizingisaprocesscomposedofaplainion-carbonitridingorion-nitridingat550~580℃,followedbyalow-temperaturechromizinginasalt-bathof590℃.ThemicrostructureandpropertiesofthelowtemperaturecompositechromizedlayeronH13toolsteelwereinvestigatedusingmetallography,X-raydiffraction,microanalysis,hardnessandweartests.Itwasfoundthatthislowtemperatureprocesswasthermodynamicallyandkineticallypossible,andthecompositechromizedlayeronH13steel,withathicknessof3~6μm,consistedofthreesub-layers(bands),viz.theouterCr-richone,theintermediate(black)one,andtheinner,originalwhitelayer.Afterchromizing,theformerdiffusionlayerwasthickened.TheresultsofX-raydiffractionshowedthatthecompositechromizedlayercontainedsuchnitridesandcarbidesofchromiumasCrN,Cr2N,(Cr,Fe)23C6,and(Cr,Fe)7C3,aswellasplainα-(Fe,Cr).Ahighsurfacemicrohardnessof1450~1550HV0.025,whichismuchhigherthanthatobtainedbytheconventionalioncarbonitridingandionnitriding,wasobtained.Inaddition,anexcellentwearresistancewasgainedonthecompositechromizedlayer.
简介:Thenon-isothermalcrystallizationkineticsofpolyamide6/diamine-modifiedmulti-walledcarbonnanotube(PA6/D-MWNT)nanocompositewasinvestigatedbydifferentialscanningcalorimetry(DSC).ThemodifiedAvramiequation,theOzawaequationandthecombinedAvrami/Ozawaequationwereemployedtoanalyzethenon-isothermalcrystallizationdata.ThecrystallizationactivationenergieswerealsoevaluatedbytheKissingermethod.ItwasfoundthatthecombinedAvrami/Ozawaequationcouldsuccessfullydescribethenon-isothermalcrystallizationprocess.TheresultsshowedthatD-MWNTsnotonlyactedaseffectivehetero-geneousnucleatingagentsforPA6andnoticeablyincreasedthecrystallizationtemperatureofPA6,butalsoinfluencedthemechanismofnucleationandcrystalgrowthofPA6andthenreducedtheoverallcrystallizationrateoftheneatPA6matrix.ThecrystallizationactivationenergyforthenanocompositesamplewasgreaterthanthatoftheneatPA6,whichindicatedthattheadditionofD-MWNTshinderedthemobilityofPA6chainsegments.
简介:微观结构和Ni//3艾尔的机械性质基于拥有低杂质内容的Ni-Al-Mosuperalloy-IC6,由水花免职技术的高密度被学习了。结果显示IC6合金在空间和中间的温度两个都有好张力的力量和延伸。(编辑作者摘要)6个裁判员。
简介:Ionbeamenhanceddeposition(IBED)wasemployedtoincreasethefrettingfatigueresistanceofTi6AI4V.CrNandTiNhardcoatingswereappliedonthebasematerialandshotpeeningwascombinedwiththehardcoatingstostudytheduplexeffectonfrettingfatigueresistance,TheIBEDcoatingsexhibitedagoodbondingstrength.Theydidnotspalloffevenaftershotpeening.However,anoptimumcompositionofCrNshowedbetterfrettingfatigueresistancethanthatofTiNwiththesameprocessingparameters.
简介:Becauseoftheexcellentmechanicalpropertiesof34C「NiMo6steel,itiswidelyusedinhigh-valuecomponents.Manyconventionalapproachestostrengthening-steelstypicallyinvolvethelossofusefulductility.Inthisstudy,34CrNiMo6Steelhavinghighstrengthandductilityisproducedbylasersolidforming(LSF)w让haquenching-tempering(QT)treatment.TemperingofbainiteismainlybysolidphasetransformationinthepreviousLSFlayersduringtheLSFprocess.ThestablemicrostructureofLSFconsistsofferriteandfinecarbides.Themicrostructuretransferstotemperedsorbiteafterheat-treatment.ThetensilepropertiesoftheLSFsteelmeetthoseofthewroughtstandard.TheUTSandelongationofLSFsampleat858MPa,19.2%,respectively,aregreaterthanthoseofthewrought.TheQTtreatmentenhancedtheultimatetensilestrengthandyieldstrengthoftheLSFsample.Theultimatetensilestrength,yieldstrength,reductioninarea,andelongationoftheLSF+QTsampleat980MPa,916MPa,58.9%,and13.9%,respectively,aregreaterthanthoseofthewroughtstandard.TheyieldstrengthoftheLSF+QTsampleisapproximately1.27timesthatofthewrought.TheLSFsamplesfailedinaductilefracturemode,whiletheLSF+QTsamplesshowedmixed-modefailure.ThedefectshaveonlyasmalleffectonthetensilepropertiesowingtotheexcellentductilityoftheLSFsample.
简介:AnewcompoundK6Ti0.67Nb15.33O42waspreparedforthefirsttimebysolidstatereactioninK2O-Ni2O3-Nb2O5ternarysystem.Thenewcompoundwascharacterizedbyelectronprobe,X-raypowderdiffractionandDTA.TheresultofX-raypowderdiffractionshowsthatK6Ti0.67Nb15.33O42crystallizesthehexagonalsystemwithunitcellparametersa=9.1341(5)A,c=12.090(1)A.andspacegroupP62/mcm(193).
简介:采用单辊法制备了宽20mm、厚25μm的Fe78Si9B13合金带材,用绕带机将其绕制成环型磁芯,然后将磁芯进行退火处理,结果表明,随着退火温度的升高,Fe78Si9B13非晶磁芯的初始磁导率m、饱磁感应强度Bs和矫顽力Hc呈先增大后减小的趋势,当退火温度达到450℃时,磁化曲线呈现出一定的线性关系,即恒导磁特性。将经4500(=/100min退火的Fe78Si9B13非晶磁芯用环氧树脂进行封装后,环氧封装后μi和Bs减小,而Hc和损耗Ps增大,磁化曲线和损耗曲线的形状与封装前相同。
简介:双相不锈钢1Cr18Ni11Si4AlTi由前苏联研制,目前在我国某些特殊行业中有重要的作用。根据我国现有标准GJB2294—95和GB/T1220—92组织生产,发现按标准中现行成分设计、热处理制度生产的产品与标准要求的力学性能(屈服强度σ0.2)需达到的规定值存在较大差异,很难达到所需要的屈服强度。通过完善相关成分和工艺参数,获得了满意的金相组织和优良的综合力学性能。通过试验探讨了生产实际与标准中的部分规定存在的差距。