Preparation of Immobilized ε-Polylysine PET Nonwoven Fabrics and Antibacterial Activity Evaluation

(整期优先)网络出版时间:2011-04-14
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Anovelantibacterialmaterial(L-PET)waspreparedbyimmobilizingε-polylysineonpolyethyleneterephthalate(PET)nonwovenfabrics.SurfacemodificationsofthefabricwereperformedbyusingachemicalmodificationprocedurewherecarboxylgroupswerepreparedonthePETsurface,acouplingagentwasgrafted,andtheε-polylysinewasimmobilized.Scanningelectronmicroscopy(SEM)wasusedtoanalyzethesurfacemorphologyofthefabrics,whilethetoluidinebluemethodandX-rayphotoelectronspectroscopy(XPS)wereusedtoevaluatethegraftingdensities.TheantibacterialactivitiesoftheL-PETwereinvestigatedbyusingtheshaking-flaskmethod.TheelectronmicrographsshowedthatthesurfaceoftheblankPETandthemodifiedfabricsdidnotchange.TheresultsofXPSanalysisconfirmedthatε-polylysinewassuccessfullygraftedontothesurfaceofPET.TheresultsoftheantibacterialexperimentsshowedthatL-PETfabricshadexcellentantibacterialactivityagainstEscherichiacoliandStaphylococcusaureus,andthatL-PETfabricswerestableinstorageforatleasttwoyears.